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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2372340Generated: October 30, 2026

Diethyl Sulfate → HCID 13853879, compound

https://huagongshe.com/reaction/2372340

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl SulfateHCID 6163—
ReactantHCID 13853865HCID 13853865—
ProductHCID 13853879HCID 13853879—

Reaction Steps

The compounds as identified in Table 12 were prepared in the synthetic manner and after-treatment similar to those in Example 5 except that the carboxylic acids with Y1, Y2, Y3, R1, R2 and R3 as identified in Table 12 were used instead of the starting 4-chloro-5-(4-carboxybenzylamino)-2-t-butyl-3(2H)pyridazinone used in Example 5. For the preparation of Compound No. 52, diethyl sulfate was used as an esterifying agent. In the NMR data, only the characteristic absorptions are given in Table 12.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05098900
Source datasetuspto-grants-1992_03
ORD IDord-0e0dc27573624cb581aba73b8e62de39
Source noteuspto-grants-1992_03