HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → 4-Ethyl-5-(4-methylbenzylamino)-2-t-butyl-3(2H)pyridazinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 4-Methylbenzylamine | HCID 66035 | — |
| Reactant | 2-t-butyl-5-chloro-4-ethyl-3(2H)-pyridazinone | HCID 13825010 | — |
| Product | 4-Ethyl-5-(4-methylbenzylamino)-2-t-butyl-3(2H)pyridazinone | HCID 13853890 | — |
Reaction Steps
The compound as identified in Table 14 was prepared in the synthetic manner and after-treatment similar to those in Example 7 except that the 4-alkyl-5-chloro-2-alkyl-3(2H)pyridazinone with R1 and R2 as identified in Table 14 was used instead of the starting 4-ethyl-5-chloro-2-t-butyl-3(2H)pyridazinone used in Example 7, and the benzylamine derivative with R3, Y1, Y2 and Y3 as identified in Table 14 was used instead of the starting 4-methylbenzylamine. In the NMR data, only the characteristic absorptions were given in Table 14.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05098900 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-a1bcb333fa1f4485af4f9c67115e435f |
| Source note | uspto-grants-1992_03 |