HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 67798788, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 67798347 | HCID 67798347 | — |
| Product | HCID 67798788 | HCID 67798788 | 90% |
Reaction Steps
Using the procedure described in Example 1, (3RS,4SR)-3-hydroxy-4-methoxy-4-[3-(naphth-2-ylmethoxy)phenyl]tetrahydropyran [Example 7, Compound No. 3] was reacted with methyl iodide to give (3RS,4SR)-3,4-dimethoxy-4-[3-(naphth-2-ylmethoxy)phenyl]tetrahydropyran (90%), m.p. 131°-133° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05098930 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-694825ce56844d1594245ca32d644594 |
| Source note | uspto-grants-1992_03 |