Triethyl phosphite → HCID 12728633, compound

HRID 2372683Notes

Reaction equation

HRID 2372683 reaction equation
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH:7]=[O:8])=[CH:5][C:4]=1[CH2:11]Cl.[P:13]([O:20]CC)([O:17][CH2:18][CH3:19])[O:14][CH2:15][CH3:16]>>[CH2:15]([O:14][P:13]([CH2:11][C:4]1[CH:5]=[C:6]([CH:7]=[O:8])[CH:9]=[CH:10][C:3]=1[O:2][CH3:1])(=[O:20])[O:17][CH2:18][CH3:19])[CH3:16]

Participants

3

Reactant 2

HCID 31215Triethyl phosphiteHCID 104237Benzaldehyde, 3-(chloromethyl)-4-methoxy-

Product 1

HCID 12728633HCID 12728633, compound

Procedure

In a ratio of 1:1 4-methoxy-3-chloromethylbenzaldehyde and triethyl phosphite were heated together until no more gas evolved. The reaction solution was then vacuum distilled to give the desired product. bp 172°-174° C. at 1 mm Hg.

Workup

  1. distillationvacuum distilled

Sources & evidence

ORD record
ord-9a9acddf20eb445f90b705bca0b40b02
Source dataset
uspto-grants-1992_03
Patent number
US05100654

Reaction notes

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