HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → HCID 12728633, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | Benzaldehyde, 3-(chloromethyl)-4-methoxy- | HCID 104237 | — |
| Product | HCID 12728633 | HCID 12728633 | — |
Reaction Steps
In a ratio of 1:1 4-methoxy-3-chloromethylbenzaldehyde and triethyl phosphite were heated together until no more gas evolved. The reaction solution was then vacuum distilled to give the desired product. bp 172°-174° C. at 1 mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05100654 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-9a9acddf20eb445f90b705bca0b40b02 |
| Source note | uspto-grants-1992_03 |