Triethyl phosphite → HCID 15045714, compound

HRID 2372684Notes

Reaction equation

HRID 2372684 reaction equation
[CH2:1]([O:3][C:4]1[CH:11]=[CH:10][C:7]([CH:8]=[O:9])=[CH:6][C:5]=1[CH2:12]Cl)[CH3:2].[P:14]([O:21]CC)([O:18][CH2:19][CH3:20])[O:15][CH2:16][CH3:17]>>[CH2:16]([O:15][P:14]([CH2:12][C:5]1[CH:6]=[C:7]([CH:8]=[O:9])[CH:10]=[CH:11][C:4]=1[O:3][CH2:1][CH3:2])(=[O:21])[O:18][CH2:19][CH3:20])[CH3:17]

Participants

3

Reactant 2

HCID 31215Triethyl phosphiteHCID 15045713HCID 15045713, compound

Product 1

HCID 15045714HCID 15045714, compound

Procedure

4-Ethoxy-3-chloromethylbenzaldehyde and triethyl phosphite were added together in a 1:1 ratio and heated until no more gas evolved. The reaction solution was then vacuum distilled to give the desired product. bp 170°-171° C. at 0.75mm Hg.

Workup

  1. temperatureheated until no more gas
  2. distillationvacuum distilled

Sources & evidence

ORD record
ord-94c3aeebbca44eb79c4b0d16389cacdf
Source dataset
uspto-grants-1992_03
Patent number
US05100654

Reaction notes

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