HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethyl phosphite → HCID 15045714, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | HCID 15045713 | HCID 15045713 | — |
| Product | HCID 15045714 | HCID 15045714 | — |
Reaction Steps
4-Ethoxy-3-chloromethylbenzaldehyde and triethyl phosphite were added together in a 1:1 ratio and heated until no more gas evolved. The reaction solution was then vacuum distilled to give the desired product. bp 170°-171° C. at 0.75mm Hg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05100654 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-94c3aeebbca44eb79c4b0d16389cacdf |
| Source note | uspto-grants-1992_03 |