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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 237270Generated: October 29, 2026

Potassium Carbonate → HCID 86657060, compound

https://huagongshe.com/reaction/237270

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantHCID 67346581HCID 67346581—
SolventMethanolHCID 887—
ProductHCID 86657060HCID 86657060—

Reaction Conditions

Temperature100 °C

Reaction Steps

The title compound of Step A was dissolved into MeOH (2 mL), then NH2OH HCl (1 mmol) and K2CO3 (2 mmol) were added. The mixture was heated at 100° C. using a microwave reactor for 1 h. The mixture was cooled to rt and purified by PTLC providing the title compound (120 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08642583B2
Source datasetuspto-grants-2014_02
ORD IDord-bbe6be8281f644f18a4cc4d24bf0bc43
Source noteuspto-grants-2014_02