Triethylamine → HCID 19902255, compound

HRID 2372756Notes

Reaction equation

HRID 2372756 reaction equation
C1(C)C=CC(S(O[CH:11]2[CH2:19][C:18]3[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=3)[CH2:12]2)(=O)=O)=CC=1.C1C2C(=CC=CC=2)CC1O.[F:31][C:32]1[CH:46]=[CH:45][C:35]2[C:36]([CH:39]3[CH2:44][CH2:43][NH:42][CH2:41][CH2:40]3)=[N:37][O:38][C:34]=2[CH:33]=1.C(N(CC)CC)C>C1(C)C=CC=CC=1>[F:31][C:32]1[CH:46]=[CH:45][C:35]2[C:36]([CH:39]3[CH2:40][CH2:41][N:42]([CH:11]4[CH2:12][C:13]5[C:18](=[CH:17][CH:16]=[CH:15][CH:14]=5)[CH2:19]4)[CH2:43][CH2:44]3)=[N:37][O:38][C:34]=2[CH:33]=1

Participants

6

Reactant 4

HCID 8471TriethylamineHCID 779362-IndanolHCID 8494213-(4-Piperidyl)-6-fluoro-1,2-benzisoxazoleHCID 70214742-Indanyl p-toluenesulfonate

Product 1

HCID 19902255HCID 19902255, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

0.173 mole of 2-indanyl para-toluenesulfonate (prepared from 2-indanol according to the procedure described in Example 4, stage B), 0.173 mole of 6-fluoro-3-piperid-4-yl-1,2-benzisoxazole, dissolved in 50 ml of toluene, and 0.0346 mole of triethylamine are mixed.

Sources & evidence

ORD record
ord-8b59cddc7ce049c2b4d5229236ffa5af
Source dataset
uspto-grants-1992_03
Patent number
US05100902

Reaction notes

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