HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 19902347, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Benzonitrile, 4-[(4-methoxyphenyl)thio]- | HCID 11172528 | — |
| Reactant | Magnesium 2-(dioxidan-2-ide-1-carbonyl)benzoate--water (1/1/6) | HCID 21894687 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19902347 | HCID 19902347 | 77% |
Reaction Steps
6 g (0.0248 mol) of 4-[(4-methoxyphenyl)thio]benzonitrile and then 18.45 g of magnesium monoperoxyphthalate hexahydrate are added to a mixture of 120 ml of ethanol and 12 ml of water. The reaction medium is kept at 40° C. for 20 minutes. After hydrolysis in iced water, the solution is filtered and the white solid is washed with water. 5.2 g (yield: 77%) of the expected product are thus obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05100913 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-677cfcaec45047f78c39ad71a87fc053 |
| Source note | uspto-grants-1992_03 |