HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl (ethoxymethylene)malonate → HCID 9980359, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl (ethoxymethylene)malonate | HCID 6871 | — |
| Reactant | HCID 178446843 | HCID 178446843 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 9980359 | HCID 9980359 | — |
Reaction Steps
The title compound is prepared form N-(2'-t-butoxycarbonylbiphen-4-yl)methylvaleramidine and diethyl ethoxymethylenemalonate (Aldrich) similarly to that in Example 7. The t-butyl ester is hydrolyzed in neat trifluoroacetic acid to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05100897 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-94cefef9de104fb0b10b7439247abbc5 |
| Source note | uspto-grants-1992_03 |