HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → 2-n-Butyl-4-chloro-5,6-dimethylpyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | 2-n-Butyl-5,6-dimethylpyrimidin-4(3H)-one | HCID 135625454 | — |
| Product | 2-n-Butyl-4-chloro-5,6-dimethylpyrimidine | HCID 19902230 | — |
Reaction Steps
The pyrimidine from Example 2 2-n-butyl-5,6-dimethylpyrimidin-4(3H)-one is converted to the title compound upon treatment with phosphoryl chloride as described by Gabriel and Colman (Ber. 1899, 32, 2921) and by Marshall and Walker (J. Chem. Soc., 1951, 1004).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05100897 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-0c1ba5391b0e4101b903f99227f3be8c |
| Source note | uspto-grants-1992_03 |