HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Acetate → HCID 14745924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | HCID 19902725 | HCID 19902725 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 14745924 | HCID 14745924 | 118.7% |
Reaction Steps
26.9 g (0.1 mol) of diisopropyl dichloromaleate, 19.27 g (0.25 mol) of ammonium acetate and 40 ml of dimethylformamide were reacted under the same conditions as described in Example 1. 29.65 g (85.6% yield) of diisopropyl aminochloromaleate were obtained as a reddish-yellow, viscous liquid (purity according to GC analysis 83%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05101067 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-70f4b319e7f645c79346629a4a3d254a |
| Source note | uspto-grants-1992_03 |