HRID2372974

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11591

Mercuric cyanide

C2HgN2

2 次

结构：CC(=O)O[C@@H]1[C@@H](OC(C)=O)[C@@H](Br)SC[C@H]1OC(C)=O

HCID10926314

未命名化合物

HCID15198240

未命名化合物

PRODUCTS

生成物

结构：COc1cc(S[C@@H]2SC[C@@H](OC(C)=O)[C@H](OC(C)=O)[C@H]2OC(C)=O)cc(OC)c1OC

HCID14795351

未命名化合物

收率 28%

PROCEDURE

实验过程

If the procedure described in Preparation I is followed starting from 11.35 g (57.10-3 mol) of 3,4,5-trimethoxybenzenethiol, 14.32 g (57.10-3 mol) of mercuric cyanide, Hg(CN)2, and 22.15 g (62.10-3 mol) of 2,3,4-tri-O-acetyl-5-thio-α-D-xylopyranosyl bromide, 7.52 g (yield: 28%) of the expected product are obtained.

WORKUP

后处理

customIf the procedure described in Preparation I