Toluene → HCID 14678244, compound

Participants

Reaction Steps

The same procedure as in Production example 27 was repeated except that 59.6 g of a toluene solution containing 41.6% of 2-methyl-3-(4-trifluoromethylphenylthio)propanal was used in place of the toluene solution containing 3-(4-trifluoromethylphenylthio)butanal. Thus, 36.67 g of crude 4-hydroxy-5-methyl-6-(4-trifluromethylphenylthio)-2-hexanone were obtained (purity: 59.3%, yield: 71.1%).

Provenance & Evidence