HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthaldehyde → HCID 19902783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthaldehyde | HCID 6195 | — |
| Reactant | 1-Acetylnaphthalene | HCID 13663 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19902783 | HCID 19902783 | — |
Reaction Steps
1-Acetonaphtone is reacted with 1-naphtoaldehyde and sodium hydroxide in ethanol to produce 1,3-dinaphthyl-3-hydroxypropanone. The resulting compound is reacted with KHSO4 to obtain 1,3-dinaphthyl-3-propene-1-on. The resulting compound is reacted with hydrazine and potassium hydroxide in triethylene glycol to produce 1,3-dinaphthylpropane. 1,3-Dinaphthylpropane is reacted with fuming nitric acid and acetic acid anhydride to produce 1,3-dinitronaphthylpropane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05101411 |
| Source dataset | uspto-grants-1992_03 |
| ORD ID | ord-50916772d7a8457ab9e81ad2d578e2e2 |
| Source note | uspto-grants-1992_03 |