HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178504267, compound → HCID 11450662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178504267 | HCID 178504267 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 11450662 | HCID 11450662 | — |
Reaction Steps
A mixture of 0.035 g of 2-Trimethylsilylethoxymethyl-5-[2′-(Phenyl)biphenyl-3-yl]-1,2,4-triazole-3-carboxamide in 3 mL of acetonitrile and 9 mL of a 50% solution of HF in water was stirred at rt for 6 hours. The reaction mixture was then concentrated and the residue was purified by chromatography (silica, CH3OH: CH2Cl2 0-5% gradient) to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07459475B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-f7ae981f71e14b1f9fb3103692dc32fa |
| Source note | uspto-grants-2008_12 |