HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 59851175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 66934950 | HCID 66934950 | — |
| Reactant | HCID 178512548 | HCID 178512548 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59851175 | HCID 59851175 | — |
Reaction Steps
In a manner similar to method I (DMF and NaHCO3 were used in place of EtOH and KCO3), 8-chloro-4-dimethylaminomethylene-1-phenyl-3,4-dihydro-1H-benzo[b]azepine-2,5-dione (v-i) and 4-guanidinobenzoic acid were converted to I-10 (61%): HRMS Calcd. for C25H17ClN4O3: 457.1067, Found 457.1076.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07459448B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-532b502d5d194b439d4d4e7ec82b9377 |
| Source note | uspto-grants-2008_12 |