huagongshe.com
HRID2373371

反应详情

EQUATION

反应方程式

HRID 2373371 的结构方程式

REACTANTS

反应物

4
结构：CN(C)C=O
HCID6228

N,N-Dimethylformamide

C3H7NO

结构：O=C([O-])O.[Na+]
HCID516892

Sodium Bicarbonate

CHNaO3

结构：CN(C)C=C1CC(=O)N(c2ccccc2)c2cc(Cl)ccc2C1=O
HCID66934950

未命名化合物

结构：N=C(N)Nc1ccc(C(=O)O)cc1
HCID178512548

未命名化合物

PRODUCTS

生成物

1
结构：O=C(O)c1ccc(Nc2ncc3c(n2)-c2ccc(Cl)cc2N(c2ccccc2)C(=O)C3)cc1
HCID59851175

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

In a manner similar to method I (DMF and NaHCO3 were used in place of EtOH and KCO3), 8-chloro-4-dimethylaminomethylene-1-phenyl-3,4-dihydro-1H-benzo[b]azepine-2,5-dione (v-i) and 4-guanidinobenzoic acid were converted to I-10 (61%): HRMS Calcd. for C25H17ClN4O3: 457.1067, Found 457.1076.