HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodoanisole → 7-(4-Methoxy-phenylethynyl)-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodoanisole | HCID 69676 | — |
| Reactant | 7-Ethynyl-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine | HCID 59852695 | — |
| Product | 7-(4-Methoxy-phenylethynyl)-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine | HCID 11392678 | — |
Reaction Steps
The title compound is prepared in analogy to example 1 from 7-ethynyl-3,3-dimethyl-3,4-dihydro-2H-benzo[b][1,4]dioxepine (6) (example 1d) and 1-iodo-4-methoxy-benzene. MS (ESI) 308.2 (M•)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07459480B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-94593c9aa7b7429eba72c4216269c73f |
| Source note | uspto-grants-2008_12 |