HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 4-iodo-N,N-dimethylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Iodobenzoyl chloride | HCID 74373 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 4-iodo-N,N-dimethylbenzamide | HCID 879933 | — |
Reaction Steps
The title compound is prepared in analogy to example 16a from 4-iodobenzoyl chloride, N,N-dimethylamine and triethylamine in CH2Cl2 as a yellowish oil, MS (ESI) 276.0 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07459480B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-0d0247903d2a4ab5b0fc147926d634e7 |
| Source note | uspto-grants-2008_12 |