HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Ethynylphenyl)(morpholino)methanone → 4-ethynyl-N,N-dimethylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Ethynylphenyl)(morpholino)methanone | HCID 57764578 | — |
| Reactant | N,N-Dimethyl-4-trimethylsilanylethynyl-benzamide | HCID 69292322 | — |
| Product | 4-ethynyl-N,N-dimethylbenzamide | HCID 20253928 | — |
Reaction Steps
The title compound is prepared in analogy to (4-ethynyl-phenyl)-morpholin-4-yl-methanone (Example 16c) from N,N-Dimethyl-4-trimethylsilanylethynyl-benzamide. 1H-NMR (300 MHz): 3.15 (s, 1H); 3.33-3.94 (br, 8H); 7.37 (d, J=6.6, 2H); 7.53 (d, J=6.6, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07459480B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-8acb0c8525174fe0b6f79586e98d9c99 |
| Source note | uspto-grants-2008_12 |