HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10616500, compound → HCID 10612438, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10616500 | HCID 10616500 | — |
| Solvent | TFA dichloromethane water | HCID 18672661 | — |
| Product | HCID 10612438 | HCID 10612438 | — |
Reaction Steps
7-benzyl 1-tert-butyl 7-azabicyclo[2.2.1]heptane-1,7-dicarboxylate (C-34)(synthesized following the procedure reported in J. O. C, 1996, 61, 6313-6325) was stirred in TFA/DCM/H2O (95/5/5, 0.3 M) for 10 minutes. Evaporation of the solvent afforded the titled compound (C-35).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07459452B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-c5c8d69178ad4d248625415f7525a18c |
| Source note | uspto-grants-2008_12 |