HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 11483844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 11694427 | HCID 11694427 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 11483844 | HCID 11483844 | — |
Reaction Steps
The 2-amino-4-chloro-thieno[2,3-d]pyrimidine-6-carboxylic acid methyl ester (100 mg, 0.39 mmol), benzylamine (100 μl) in 4 mL of THF are submitted to MW irradiation at 110° C. for 35 mins. The reaction was cooled to room temperature and worked up (acidic) and purified using standard conditions for a neutral compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642594B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-9fbcb7ba74424b3aba493cef24ab06c0 |
| Source note | uspto-grants-2014_02 |