HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 3730311, compound → HCID 72818345, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 3730311 | HCID 3730311 | — |
| Reactant | HCID 53436803 | HCID 53436803 | — |
| Product | HCID 72818345 | HCID 72818345 | — |
Reaction Steps
The title compound was prepared from 4-(5-trifluoromethyl-pyridin-2-yloxy)-benzoic acid (283 mg, 1.0 mmol) and 2-amino-3-(4′-trifluoromethyl-biphenyl-4-yl)-propionic acid methyl ester (360 mg, 1.0 mmol) following general procedure A. (580 mg) 1H-NMR(400 MHz, CD3COCD3): 3.24 (dd, 1H), 3.39 (dd, 1H), 3.74 (s, 3H), 4.98 (m, 1H), 6.64 (d, 1H), 7.50 (m, 2H), 7.60 (m, 2H), 7.69 (m, 3H), 7.78 (d, 2H), 7.88 (d, 2H), 7.98(m, 2H), 8.15 (m, 2H); LC/MS (m/z): 589 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07459472B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-ec57ca60e8fd40c6a9b9b2e249b0f5c6 |
| Source note | uspto-grants-2008_12 |