Ammonium Chloride → HCID 59853022, compound

Participants

Reaction Steps

The title compound was prepared by the reduction of tert-butyl(1-(3-(4-(2-fluoro-4-nitrophenoxy)pyridin-3-yl)prop-2-ynyl)azetidin-3-yl)methylcarbamate (30 mg, 0.66 mmol) in the same manner as in Step E of Example 35 using Fe powder (50 g, 0.091 mmol) and NH4Cl (96 mg, 1.82 mmol). The product was used in subsequent reactions without any purification. MS(ESI+): m/z 371.24 (100), [(M-C4H9)]+; m/z 427.27 (25), (M+H)+.

Provenance & Evidence