HuagongsheHuagongshe Chemistry Print Report · For research reference only
sodium (1Z)-1-cyanoprop-1-en-2-olate → HCID 178467935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | sodium (1Z)-1-cyanoprop-1-en-2-olate | HCID 23687916 | — |
| Reactant | HCID 178519375 | HCID 178519375 | — |
| Product | HCID 178467935 | HCID 178467935 | — |
Reaction Steps
The title compound was prepared from 2.85 g (70% purity, 8.87 mmol) 3-bromo-1H-indazole-5-carbaldehyde (Example 10A) and 1.03 g (9.75 mmol) sodium (1Z)-1-cyanoprop-1-en-2-olate in analogy to the procedure described in Example 9A yielding 1.12 g (43% of th.) of product which was used in subsequent steps without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642595B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-91a338ab524f4313ac064a6b678c3af1 |
| Source note | uspto-grants-2014_02 |