Dimethyl Sulfate →

Participants

Reaction Steps

0.38 g (3 mmol) of dimethyl sulfate was added to 0.69 g (2.4 mmol) of the product from Step 2.4 in 10 mL of ethyl acetate, and the mixture was allowed to agitate overnight. A viscous oil separated. The supernatant solution was decanted and discarded. The residue was used in the next step without further purification.

Provenance & Evidence