Azobisisobutyronitrile → HCID 86609791, compound

Participants

Reaction Steps

5 g of t-butylacrylate, 2.5 g of 2-(trifluoromethyl)acrylic acid, 2.5 g of 2,2,3,4,4,4-hexafluorobutyl methacrylate and 0.2 g of AIBN were dissolved in 50 g of acetone. The monomers were polymerized at 67° C. for 6 hours. After completion of the polymerization, the polymerization product was precipitated in water, filtered, and dried in a vacuum to give poly(t-butylacrylate-2-(trifluoromethyl)acrylic acid-2,2,3,4,4,4-hexafluorobutyl methacrylate) (yield: 75%) of Formula 3, below:

Provenance & Evidence