p-(1-Piperazinyl)phenol → HCID 59853661, compound

HRID 2374267Notes

Reaction equation

HRID 2374267 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]2)=[CH:4][CH:3]=1.[CH3:14][S:15]([C:18]1[CH:19]=[C:20]([C:30](O)=[O:31])[C:21]([C:24]2[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=2)=[CH:22][CH:23]=1)(=[O:17])=[O:16]>>[OH:1][C:2]1[CH:3]=[CH:4][C:5]([N:8]2[CH2:13][CH2:12][N:11]([C:30]([C:20]3[CH:19]=[C:18]([S:15]([CH3:14])(=[O:17])=[O:16])[CH:23]=[CH:22][C:21]=3[C:24]3[CH:29]=[CH:28][CH:27]=[CH:26][CH:25]=3)=[O:31])[CH2:10][CH2:9]2)=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 92467p-(1-Piperazinyl)phenolHCID 574452544-(methylsulfonyl)-Biphenyl-2-carboxylic acid

Product 1

HCID 59853661HCID 59853661, compound

Procedure

The title compound was prepared according to the procedure E described for Example 9 from ′1-(4-hydroxyphenyl)-piperazine [56621-48-8] and 4-Methanesulfonyl-biphenyl-2-carboxylic acid (Example V). MS (ISP): 437.4 MH+.

Sources & evidence

ORD record
ord-292c8741249e493eaad6062b882988dd
Source dataset
uspto-grants-2008_12
Patent number
US07462617B2

Reaction notes

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