HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetohydrazide → HCID 178446280, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetohydrazide | HCID 229753 | — |
| Reactant | methyl 4-(pentylamino)-1H-imidazole-5-carbimidothioate | HCID 135984704 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178446280 | HCID 178446280 | — |
Reaction Steps
The mixture of methyl 4-(pentylamino)-1H-imidazole-5-carbimidothioate (0.53 g, 2.4 mmol) and trifluoroacetic acid hydrazide (0.45 g, 3.5 mmol) in ethanol (10 mL) was refluxed overnight. The reaction mixture was concentrated to yield the product as slightly green viscous oil. LCMS calculated for C11H16F3N6(M+H): 289.1; found: 289.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07462624B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-aff303fd66c948cc8dda709e1a4b0f29 |
| Source note | uspto-grants-2008_12 |