HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-3,5-dimethylphenol → 4-(4-Bromo-3,5-dimethylphenoxy)-2-methylbutan-2-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-3,5-dimethylphenol | HCID 81970 | — |
| Reactant | 2-Methyl-4-[(4-methylbenzenesulfonyl)oxy]butan-2-ol | HCID 14001295 | — |
| Product | 4-(4-Bromo-3,5-dimethylphenoxy)-2-methylbutan-2-ol | HCID 67972921 | — |
Reaction Steps
The title compound is prepared from 4-bromo-3,5-dimethylphenol and 3-hydroxy-3-methylbutyl 4-methylbenzenesulfonate following a procedure analogous to that described in Step 3 of Intermediate 2. LC (method 1): tR=1.35 min; Mass spectrum (ESI+): m/z=269 [M+H—H2O]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642585B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-e4989bf4efff40cca74e691b42b4316a |
| Source note | uspto-grants-2014_02 |