HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2,3-Dihydro-1H-indol-1-yl)ethan-1-one → HCID 21887170, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2,3-Dihydro-1H-indol-1-yl)ethan-1-one | HCID 27673 | — |
| Reactant | 5-Chlorovaleryl chloride | HCID 74089 | — |
| Product | HCID 21887170 | HCID 21887170 | 45.4% |
Reaction Steps
Using 1-acetylindoline (1.60 g) and 5-chlorovaleryl chloride (1.70 g) according to the same method as that of Reference Example 1, the title compound (1.26 g) was obtained as colorless crystals having a melting point of 90 to 91° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07462628B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-8bcfd6ca545149bb9c82879e445ab132 |
| Source note | uspto-grants-2008_12 |