5-Chlorovaleryl chloride → HCID 21887238, compound
Reaction equation
[CH2:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH2:3][CH:2]1[NH:10][C:11](=[O:13])[CH3:12].[Cl:14][CH2:15][CH2:16][CH2:17][CH2:18][C:19](Cl)=[O:20]>>[Cl:14][CH2:15][CH2:16][CH2:17][CH2:18][C:19]([C:6]1[CH:5]=[C:4]2[C:9](=[CH:8][CH:7]=1)[CH2:1][CH:2]([NH:10][C:11](=[O:13])[CH3:12])[CH2:3]2)=[O:20]Participants
3
Procedure
Using N-(2,3-dihydro-1H-inden-2-yl)acetamide and 5-chlorovaleryl chloride according to the same method as that of Reference Example 1, the title compound was obtained as colorless crystals having a melting point of 106 to 108° C.
Sources & evidence
- ORD record
- ord-179f4c0ac8bd4256b00d546e61e66a37
- Source dataset
- uspto-grants-2008_12
- Patent number
- US07462628B2
Reaction notes
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