HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 136401929, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 136181655 | HCID 136181655 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 136401929 | HCID 136401929 | 72% |
Reaction Steps
Preparation of example 178 from the title compound of Example 155 (90 mg, 0.194 mmol) and 4M HCl in dioxane (10 mL) was carried out analogously to Example 91. Isolation, also in an analogous manner afforded the title compound (56 mg, 0.140 mmol) as an orange/yellow powder in 72% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07462713B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-bbac70355dfd473289f943ac8bbd442d |
| Source note | uspto-grants-2008_12 |