HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14915848, compound → HCID 59732106, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14915848 | HCID 14915848 | — |
| Reactant | 10H-Phenothiazine-2-carboxylic acid | HCID 22711593 | — |
| Product | HCID 59732106 | HCID 59732106 | 62% |
Reaction Steps
The experimental protocol used is the same as that described for the synthesis of intermediate 1.10, using 1-(5-acetyl-10,11-dihydro-5H-dibenzo[b,f]azepin-3-yl)ethanone (J. Chem. Soc. 1973, 859-863) as starting product. A pale yellow solid is obtained with a yield of 62%. Melting point: 189-189.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465721B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-f43946deabd84345941c79cb17f72f45 |
| Source note | uspto-grants-2008_12 |