HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-3,5-dimethylphenol → 4-((4-Bromo-3,5-dimethylphenoxy)methyl)tetrahydro-2H-pyran-4-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-3,5-dimethylphenol | HCID 81970 | — |
| Reactant | 1,6-Dioxaspiro[2.5]octane | HCID 160439 | — |
| Product | 4-((4-Bromo-3,5-dimethylphenoxy)methyl)tetrahydro-2H-pyran-4-ol | HCID 86697193 | — |
Reaction Steps
The title compound is prepared from 4-bromo-3,5-dimethylphenol and 1,6-dioxaspiro[2.5]octane following a procedure analogous to that described in Step 3 of Intermediate 2. LC (method 7): tR=1.04 min; Mass spectrum (ESI−): m/z=313 [M−H]−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642585B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-3522e7585b5d4f6396a760adec6c2281 |
| Source note | uspto-grants-2014_02 |