Hydrochloric Acid → HCID 59854615, compound

Participants

Reaction Steps

To a solution of tert-butyl-3-(3,5-dioxomorpholin-4-yl)propylcarbamate (15 g) in dry ether (150 mL) was added a saturated solution of dry HCl (gas) in diethylether (300 mL) at 0° C. and the solution was then slowly warmed up to r.t. The precipitate obtained was filtered, washed with cold ether and dried under vacuum to give 11 g of the title compound (94%).

Provenance & Evidence