Sulfuric Acid → HCID 85988014, compound

Participants

Reaction Conditions

Reaction Steps

Concentrated sulfuric acid was added to a solution of 3-[(4,4-dimethoxybutyl)thio]-4-methyl-5-phenyl-4H-1,2,4-triazole (20.49 mmol, 6.30 g) in ethanol (50 ml) until cloudy. The mixture was stirred at 40° C. for 2 h and then made alkaline with sodium carbonate and subsequently extracted with ethyl acetate. The organic phase was dried and concentrated, resulting in 4.8 g of the title compound colorless oil.

Provenance & Evidence