HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Bromide → HCID 69277513, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Bromide | HCID 6332 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 69275281 | HCID 69275281 | — |
| Product | HCID 69277513 | HCID 69277513 | — |
Reaction Steps
Utilizing the general procedure outlined in Example 65, 1-[4-acetyl-1-(4-hydroxy-2-methoxy-phenyl)-2,5-dimethyl-1H-pyrrol-3-yl]-ethanone (70 mg, 2.3 mmol) reacted with bromoethane (300 μL, excess), in the presence of K2CO3 (50 mg), to afford 1-[4-acetyl-1-(4-ethoxy-2-methoxy-phenyl)-2,5-dimethyl-1H-pyrrol-3-yl]-ethanone: MS (ESI) 330 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465730B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-de3a5bfdd9fc42fda0fd3b8ff85920d9 |
| Source note | uspto-grants-2008_12 |