HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen chloride-ethyl acetate → HCID 68920400, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 68920401 | HCID 68920401 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 68920400 | HCID 68920400 | — |
Reaction Steps
To a solution of 2-acetyloxybenzoic acid 6-(nitrooxymethyl)-2-methylpyridinyl ester (1 g, 2.88 mmoles) in ethyl acetate (20 ml) cooled at 0° C., a solution of ethyl acetate/HCl 5M is added dropwise under stirring. It is left for 1 hour at 0° C., then the temperature is let reach room values. The formed precipitate is filtered and washed with ethyl ether. 900 mg of solid product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465803B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-19dc8e9d0be843928f2e192f6b323f45 |
| Source note | uspto-grants-2008_12 |