HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → 5-[(3-Methyl-3-oxetanyl)methoxy]-1,3-benzenedimethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | Dimethyl 5-((3-methyloxetan-3-yl)methoxy)isophthalate | HCID 86697232 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 5-[(3-Methyl-3-oxetanyl)methoxy]-1,3-benzenedimethanol | HCID 86697233 | — |
Reaction Steps
The title compound is prepared from dimethyl 5-((3-methyloxetan-3-yl)methoxy)isophthalate by reduction with lithium aluminum hydride in tetrahydrofuran. LC (method 7): tR=0.69 min; Mass spectrum (ESI+): m/z=239 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642585B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-1dd14025886d46be84e5b54883a36f74 |
| Source note | uspto-grants-2014_02 |