HRID2375981
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A mixture of (6-[(1-benzyl-3-pyrrolidinyl)amino]-3-pyridyl)methanol (0.96 g) and MnO2 (2.951 g) in AcOEt (50 ml) was refluxed under stirring for 1.5 hour. After removal of the insoluble material, and the solvent was evaporated in vacuo to give 6-[(1-benzyl-3-pyrrolidinyl)amino]nicotinaldehyde (0.75 g)
WORKUP
后处理
- temperaturewas refluxed
- customAfter removal of the insoluble material
- customthe solvent was evaporated in vacuo