HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68708010, compound → HCID 68706763, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68708010 | HCID 68708010 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 68706763 | HCID 68706763 | 83% |
Reaction Steps
Using N-benzyl-3-(4-isopropylphenyl)-5-methoxy-2,2,4,6-tetramethyl-2,3-dihydro-1-benzofuran-7-amine obtained in Reference Example 95, the title compound was synthesized in the same manner as in Reference Example 30. Yield 83%. Melting point: 111-112° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465815B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-4ecdd71f1c4b41959e278358b304b746 |
| Source note | uspto-grants-2008_12 |