HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2,6-dimethylpyrimidine → 4-(4-Bromo-3,5-dimethyl-phenyl)-2,6-dimethyl-pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2,6-dimethylpyrimidine | HCID 10965245 | — |
| Reactant | 2-(4-Bromo-3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane | HCID 56973136 | — |
| Product | 4-(4-Bromo-3,5-dimethyl-phenyl)-2,6-dimethyl-pyrimidine | HCID 86697307 | — |
Reaction Steps
The title compound is prepared from 2-bromo-1,3-dimethyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzene and 4-bromo-2,6-dimethyl-pyrimidine following a procedure analogous to that described in Step 1 of Intermediate 56. LC (method 7): tR=1.01 min; Mass spectrum (ESI+): m/z=291/293 (Br) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642585B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-c77bf69497f8481e8bc26f3ce54c1ded |
| Source note | uspto-grants-2014_02 |