HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68707911, compound → HCID 68707072, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68707911 | HCID 68707911 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 68707072 | HCID 68707072 | 85% |
Reaction Steps
Using N-benzyl-4,6,7-trimethyl-3-(5-methylpyridin-2-yl)-2,3-dihydro-1-benzofuran-5-amine obtained in Reference Example 278, the title compound was synthesized in the same manner as in Reference Example 30. Yield 85%. Melting point: 125-127° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465815B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-6794112c5d0946809bf1cdd1154f150d |
| Source note | uspto-grants-2008_12 |