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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2376404Generated: October 30, 2026

HCID 68711355, compound → HCID 68709946, compound

https://huagongshe.com/reaction/2376404

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 68711355HCID 68711355—
SolventHexaneHCID 8058—
ProductHCID 68709946HCID 6870994683%

Reaction Steps

Using (cis)-3-(4-isopropylphenyl)-2,4,6,7-tetramethyl-2,3-dihydro-1-benzofuran obtained in Reference Example 349, (cis)-5-bromo-3-(4-isopropylphenyl)-2,4,6,7-tetramethyl-2,3-dihydro-1-benzofuran was synthesized in the same manner as in Reference Example 23. Using this compound, (cis)-N-benzyl-3-(4-isopropylphenyl)-2,4,6,7-tetramethyl-2,3-dihydro-1-benzofuran-5-amine were synthesized in the same manner as in Reference Example 24. Using this compound, the title compound was synthesized in the same manner as in Reference Example 30. Yield 83%. Melting point: 91-92° C. (hexane).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07465815B2
Source datasetuspto-grants-2008_12
ORD IDord-02e5f97357c64364a881cd75e9d0d158
Source noteuspto-grants-2008_12