huagongshe.com
HRID23765

反应详情

EQUATION

反应方程式

HRID 23765 的结构方程式

REACTANTS

反应物

3
结构：CC(C)CN
HCID6558

Isobutylamine

C4H11N

结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=[N+]([O-])c1cnc2ccccc2c1Cl
HCID11275808

4-Chloro-3-nitroquinoline

C9H5ClN2O2

PRODUCTS

生成物

1
结构：CC(C)Cc1c([N+](=O)[O-])cnc2ccccc12
HCID22590498

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：Cc1ccccc1
溶剂HCID1140

Toluene

C7H8

PROCEDURE

实验过程

4-chloro-3-nitro-quinoline is reacted with isobutyl amine in the presence of triethylamine (TEA) at between −10 and +15° C. in toluene, while excluding moisture. After washing and phase separation, the organic solution is ready for the next step.

WORKUP

后处理

  1. washAfter washing
  2. customphase separation