HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-6-ethylpyridazine → 3-(4-Chloro-3,5-dimethyl-phenyl)-6-ethyl-pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-6-ethylpyridazine | HCID 19797309 | — |
| Reactant | 2-(4-Chloro-3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane | HCID 53217128 | — |
| Product | 3-(4-Chloro-3,5-dimethyl-phenyl)-6-ethyl-pyridazine | HCID 86697326 | — |
Reaction Steps
The title compound is prepared from 2-cloro-1,3-dimethyl-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-benzene and 3-bromo-6-ethyl-pyridazine following a procedure analogous to that described in Step 1 of Intermediate 56. LC (method 11): tR=1.00 min; Mass spectrum (ESI+): m/z=247/249 (Cl) [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08642585B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-1d7b70542c2a422cbde44f2150084c44 |
| Source note | uspto-grants-2014_02 |