HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86612365, compound → HCID 86612364, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86612365 | HCID 86612365 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 86612364 | HCID 86612364 | 98% |
Reaction Steps
Using tert-butyl (7-bromo-2,2,4,6-tetramethyl-3-oxo-2,3-dihydro-1-benzofuran-5-yl)carbamate obtained in Reference Example 66, the title compound was synthesized in the same manner as in Example 234. Yield: 98%. Melting point: 187-188° C. (ethyl acetate-hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07465815B2 |
| Source dataset | uspto-grants-2008_12 |
| ORD ID | ord-c296461f2374446a864e2db823465d46 |
| Source note | uspto-grants-2008_12 |